License: This is an open access collection distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited
Protocol status: In development
We are still developing and optimizing this protocol, but it should be functional. We hope to solicit feedback primarily on clarity and usability. We intend to publish it in June 2025.
Created: February 24, 2025
Last Modified: February 24, 2025
Collection Integer ID: 123285
Funders Acknowledgements:
National Science Foundation
Grant ID: 1946970
Abstract
The NAN Materials SSNMR Data Acquisition Protocols collection is part of the NAN Materials SSNMR Knowledgebase; a collection of resources, training and educational material, pulse programs and parameter sets, calibration procedures, sample data sets, and protocols designed to enable users with limited NMR expertise to design experiments, collect, and analyze NMR to address common research questions in materials science or chemistry using solid-state NMR. This collection includes the first batch of protocols, including both fundamental experiments (such as the quantitative Bloch decay or CPMAS) and advanced experiments (including D-HMQC and RESPDOR).
Guidelines
These protocols have been successfully tested at NMRFAM, but are still under beta testing conditions. Use care when implementing them at a local facility, and consult with a local NMR expert when in doubt. Feedback is appreciated.
Safety warnings
While the protocols warn when there is a risk of damage to the NMR probe by using high power, the associated pulse programs do not have safety interlocks; always be cautious of the power level being applied to the probe.
Before start
To access the pulse programs associated with these protocols, visit the NAN data browser at usnan.nmrhub.org and navigate to the appropriate Knowledgebase entry.
