Compound | Abbreviation | Supplier | Catalogue Number | Concentration | Storage Conditions | |
Paracetamol | APAP | Cerilliant/Merck | A-064-1ML | 1 mg/mL in MeOH | -20C | |
AT7519 | AT7519 | Astex Pharmaceuticals | /// | 1 mg/mL in MeOH | -20C | |
[2H]4-paracetamol | D4-APAP | Cerilliant/Merck | P-909-1ML | 1 mg/mL in MeOH | -20C | |
[2H]8-AT16043M | d8-AT7519 | Astex Pharmaceuticals | /// | 1 mg/mL in MeOH | -20C |
Item | Model | Manufacturer | |
Plate Shaker | Grant Scientific TS-DW Deepwell | ThermoFisher | |
Liquid Handling Robot | Extrahera | Biotage | |
Evaporator | SPE Dry-96 dual | Biotage | |
Liquid Chromatography Pump | Acquity Binary Solvent Manager | Waters | |
Column oven | Acquity Column Manager | Waters | |
Autosampler | Waters Acquity Sample Manager with Sample Organiser | Waters | |
Mass spectrometer | QTrap 5500 | AB Sciex |
Item | Supplier | Part number | |
Methanol (HPLC grade) | VWR | C-20864320-X | |
Water (HPLC grade) | Fisher Scientific UK Ltd | C-10449380-X | |
Acetonitrile (HPLC grade) | VWR | C-20060320-X | |
Water (LC-MS grade) | VWR | 83645.320 | |
Methanol (LC-MS grade) | VWR | 83638.320 | |
Acetonitrile (LC-MS grade) | VWR | 83640.320 | |
1.75mL glass vials with lids | Scientific Laboratory Supplies Ltd | TUB1200 | |
2 mL deep well 96 well collection plate | Biotage | 121-5203 | |
Biotage PPT+ plate | Biotage | 120-2040-P01 | |
96 Extrahera 1000 L pipette tips | Biotage | 414141 | |
2 mL deep well 96 well collection plate | Waters | 186002482 | |
96 well plate sealing film | VWR | 391-1250 | |
Zone-free 96 well plate sealing film | Sigma-Aldrich | Z721646-50EA | |
Waters BEH C18 100 x 2.1 mm, 1.7m LC column | Waters |