A | B | C | |
Standard | PPB | 16x PPB | |
10 | 500 | 8000 | |
9 | 250 | 4000 | |
8 | 125 | 2000 | |
7 | 62.5 | 1000 | |
6 | 31.2 | 500 | |
5 | 15.6 | 250 | |
4 | 7.8 | 125 | |
3 | 3.9 | 62 | |
2 | 2.0 | 32 | |
1 | 1.0 | 16 |
A | B | |
Injection Volume | 2 µl | |
Needle Wash | 5 seconds with Acetonitrile | |
Column Temp | 30.00 °C |
A | B | C | |
Time | A% | B% | |
0.70 min | 95% | 5% | |
1.3 min | 50% | 50% | |
8.0 min | 10% | 90% | |
10.0 min | 10% | 90% | |
12.0 min | 95% | 5% |
A | B | |
Agilent 6460C Triple Quadrupole Parameters | ||
Ionization mode | Positive ESI with Agilent Jet Stream | |
Scan type | Dynamic MRM | |
Gas temperature | 200 °C | |
Gas Flow | 8 L/min | |
Nebulizer pressure | 45 psi | |
Sheath gas temperature | 400 °C | |
Sheath gas flow | 12 L/min | |
Capillary voltage | 3000 V | |
Nozzle voltage | 500 V | |
Delta EMV | 500 | |
Cycle Time | 500 ms |
A | B | C | D | E | F | G | H | I | J | |
Compound Name | RT | Prec Ion | Prod Ion | Frag (V) | CE (V) | Cell Acc (V) | Ret window | Polarity | ION | |
1. Ergosine | 5.4 | 548.0 | 530.2 | 150 | 15 | 4 | 1 | Positive | Qual | |
1. Ergosine | 5.4 | 548.0 | 223.1 | 150 | 35 | 6 | 1 | Positive | Quant | |
1. Ergosine | 5.4 | 548.0 | 208.0 | 150 | 50 | 4 | 1 | Positive | Qual | |
2. Ergotamine | 5.7 | 582.1 | 277.1 | 140 | 25 | 6 | 1 | Positive | Qual | |
2. Ergotamine | 5.7 | 582.1 | 223.1 | 140 | 35 | 6 | 1 | Positive | Quant | |
2. Ergotamine | 5.7 | 582.1 | 208.0 | 140 | 45 | 4 | 1 | Positive | Qual | |
3. Ergocornine | 6.4 | 562.1 | 305.1 | 140 | 25 | 6 | 1 | Positive | Qual | |
3. Ergocornine | 6.4 | 562.1 | 277.1 | 140 | 30 | 4 | 1 | Positive | Qual | |
3. Ergocornine | 6.4 | 562.1 | 223.1 | 140 | 35 | 6 | 1 | Positive | Quant | |
4. Ergocryptine | 6.9 | 576.0 | 305.1 | 120 | 25 | 6 | 1 | Positive | Qual | |
4. Ergocryptine | 6.9 | 576.0 | 291.1 | 120 | 25 | 4 | 1 | Positive | Qual | |
4. Ergocryptine | 6.9 | 576.0 | 223.1 | 120 | 35 | 6 | 1 | Positive | Quant | |
5. Ergocristine | 7.1 | 610.0 | 305.0 | 140 | 25 | 4 | 1 | Positive | Qual | |
5. Ergocristine | 7.1 | 610.0 | 268.2 | 140 | 25 | 7 | 1 | Positive | Qual | |
5. Ergocristine | 7.1 | 610.0 | 223.1 | 140 | 40 | 6 | 1 | Positive | Quant | |
6. Ergosinine | 7.5 | 548.2 | 530.1 | 141 | 14 | 4 | 1 | Positive | Qual | |
6. Ergosinine | 7.5 | 548.2 | 223.1 | 141 | 34 | 5 | 1 | Positive | Quant | |
6. Ergosinine | 7.5 | 548.2 | 208.0 | 141 | 50 | 4 | 1 | Positive | Qual | |
7. Ergotaminine | 7.9 | 582.2 | 277.1 | 144 | 26 | 5 | 1 | Positive | Qual | |
7. Ergotaminine | 7.9 | 582.2 | 223.1 | 144 | 34 | 5 | 1 | Positive | Quant | |
7. Ergotaminine | 7.9 | 582.2 | 208.1 | 144 | 50 | 5 | 1 | Positive | Qual | |
8. Ergocorninine | 8.3 | 562.2 | 305.1 | 140 | 30 | 5 | 1 | Positive | Qual | |
8. Ergocorninine | 8.3 | 562.2 | 277.1 | 140 | 30 | 4 | 1 | Positive | Qual | |
8. Ergocorninine | 8.3 | 562.2 | 223.1 | 140 | 38 | 5 | 1 | Positive | Quant | |
9. Ergocryptinine | 8.9 | 576.2 | 305.1 | 138 | 30 | 5 | 1 | Positive | Qual | |
9. Ergocryptinine | 8.9 | 576.2 | 291.1 | 138 | 30 | 4 | 1 | Positive | Qual | |
9. Ergocryptinine | 8.9 | 576.2 | 223.1 | 138 | 38 | 5 | 1 | Positive | Quant | |
10. Ergocristinine | 9.1 | 610.2 | 305.1 | 139 | 30 | 5 | 1 | Positive | Qual | |
10. Ergocristinine | 9.1 | 610.2 | 268.0 | 139 | 24 | 7 | 1 | Positive | Qual | |
10. Ergocristinine | 9.1 | 610.2 | 223.1 | 139 | 38 | 5 | 1 | Positive | Quant | |
11. Dihydroergocristine | 6.6 | 612.8 | 350.1 | 178 | 26 | 4 | 1 | Positive | Quant | |
11. Dihydroergocristine | 6.6 | 612.8 | 270.1 | 178 | 34 | 4 | 1 | Positive | Qual | |
11. Dihydroergocristine | 6.6 | 612.8 | 253.1 | 178 | 38 | 4 | 1 | Positive | Qual |
A | B | C | D | E | F | G | |
# | Start time | Scan type | Div Valve | Delta EMV (+) | Delta EMV (-) | Stored | |
1 | 0 | Dynamic MRM | To MS | 500 | 0 | x | |
2 | 10 | Dynamic MRM | To Waste | 0 | 0 | x |